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Martensitic Transformation in Nanostructured NiTi Alloy Studied by X-ray Diffraction In-Situ Heating

dc.contributor.authorSwiec, Pawel
dc.contributor.authorZubko, Maciej Jan
dc.contributor.authorStroz, Danuta
dc.contributor.authorLekston, Zdzislaw
dc.date.accessioned2026-08-18T12:31:41Z
dc.date.issued2019
dc.description.abstractIn this work martensitic transformation of Ni-rich NiTi alloy subjected to 17, 20 and 35% cold-rolling in the martensitic state followed by annealing at 450 degrees C for 15 min has been studied by in-situ X-ray Diffraction, Transmission Electron Microscopy and Differential Scanning Calorimetry. It has been found that the material after thermo-mechanical treatment has ultra-fine grained structure with small number of large grains with high dislocation density. Phase composition of that nanostructured alloy consists of B2 austenite, B19' martensite and R rhombohedral phases. B2 and B19' were stable at high as well as at low temperatures. DSC measurements revealed that the studied material shows multistage character of phase transformation. Therefore it was decided to adopt in-situ XRD analysis.eng
dc.description.abstract-translatedIn this work martensitic transformation of Ni-rich NiTi alloy subjected to 17, 20 and 35% cold-rolling in the martensitic state followed by annealing at 450 degrees C for 15 min has been studied by in-situ X-ray Diffraction, Transmission Electron Microscopy and Differential Scanning Calorimetry. It has been found that the material after thermo-mechanical treatment has ultra-fine grained structure with small number of large grains with high dislocation density. Phase composition of that nanostructured alloy consists of B2 austenite, B19' martensite and R rhombohedral phases. B2 and B19' were stable at high as well as at low temperatures. DSC measurements revealed that the studied material shows multistage character of phase transformation. Therefore it was decided to adopt in-situ XRD analysis.cze
dc.event12th Japanese-Polish Joint Seminar on Micro and Nano Analysis (29.08.2018 - 01.09.2018, Kyushu)eng
dc.formatp. 708-713
dc.identifier.doi10.2320/matertrans.MC201808
dc.identifier.issn1345-9678
dc.identifier.obd43875230
dc.identifier.scopus2-s2.0-85065410045
dc.identifier.urihttps://hdl.handle.net/20.500.12603/3151
dc.identifier.wos000465516200015
dc.language.isoeng
dc.peerreviewedyes
dc.publicationstatuspostprint
dc.publisherJAPAN INST METALS & MATERIALS
dc.relation.ispartofMATERIALS TRANSACTIONS, volume 60, issue: 5eng
dc.relation.publisherversionhttps://www.jstage.jst.go.jp/article/matertrans/60/5/60_MC201808/_pdf/-char/en
dc.rights.accessOpen Access
dc.rights.licenseCC BY
dc.source.urlhttps://www.jstage.jst.go.jp/article/matertrans/60/5/60_MC201808/_pdf/-char/en
dc.subjectnanostructured materialseng
dc.subjectnickel titanium shape memory alloyeng
dc.subjectsevere cold-rollingeng
dc.subjectin-situ X-ray diffractioneng
dc.subjectmartensitic transformationeng
dc.subjectnanostrukturované materiálycze
dc.subjectslitina niklu titanu s tvarovou pamětícze
dc.subjecttěžké válcování za studenacze
dc.subjectin-situ rentgenová difrakcecze
dc.subjectmartenzitická transformacecze
dc.titleMartensitic Transformation in Nanostructured NiTi Alloy Studied by X-ray Diffraction In-Situ Heatingeng
dc.title.alternativeMartenzitická transformace v nanostrukturované slitině NiTi pomocí rentgenovské difrakcecze
dc.typearticle

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